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Advance Gas Chromatography Operation, Calibration, Troubleshooting & Practice

ENDED
Short Course by  EcoMan
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On-Site / Short Course

Details

This course is designed to integrate the various aspects and techniques within the field of separation science. We will cover theory, instrumentation, and practice of modern separation techniques including gas chromatography, liquid chromatography, and electro kinetic separations. We will also discuss sample preparation methods. The emphasis of the course is on practical, empirical, and applied aspects of the above, with sufficient coverage of theory to provide a thorough understanding of how the methods work and to facilitate method development. The unifying features of the various separations techniques are, not surprisingly, the fundamental physical parameters governing the separative process - including equilibrium, mass transport, bulk fluid transport, zone formation and perturbation, etc. These unifying features will guide us through the course.

Outline

• Introduction to separation science
• Separations theory and calculations
• Column Systems
- Packed and capillary
- Performance evaluations, how they are made
- Liquid phases/selection/temperature limits
- Solid supports
- Adsorbents, molecular sieves
- How to select the type of columns required for plant application
- Isothermal/temperature programming
- Compatibility, operating tips
- Installation of columns, trouble-shooting, gas flow adjustments
- Linear velocity thru capillary column
- Operational tips
- Column behavior
- Maintenance and trouble-shooting
• Gas chromatography: hardware and methods
• High performance liquid chromatography: hardware and methods
• Introduction to modern electrophoretic methods of analysis
• Sample preparation • Biological, environmental, and industrial applications (interspersed among the above)
• Introduction to Troubleshooting and Preventive Maintenance • System Familiarization
• Inlet Troubleshooting and Maintenance
• Worksheet Exercise 1
• Automatic Liquid Sampler (ALS) Troubleshooting and Maintenance
• Capillary Column Troubleshooting and Maintenance
• Video Segment 2: Column Installation
• Electronic Pneumatic Control (EPC) T&M
• Detector Troubleshooting and Maintenance
• Worksheet Exercise 2
• Worksheet Exercise 3
• Data System Troubleshooting and Conclusion
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